NMR facility

Solid state NMR

Shared probeheads on both units:

  • 1,3mm HXY (X=13C–31P ; Y=183W–11B) ;
  • 2,5mm :
    • HX (1H–19F ; X=113In–31P) ;
    • HXY (X=29Si–31P ; Y=47Ti–87Rb) ;
  • 3,2mm HXY (X=111Cd–31P ; Y=67Zn–141Pr) ;
  • 4mm :
    • HX (X=207Pb–31P),
    • HX MQMAS (X=29Si–119Sn),
    • HX (X=105Pd–13C),
    • HX (101Ru–31P), WVT, T° : -60°C +300°C,
    • HX (X=75As–31P ; Y=25Mg–119Sn) ;
  • 5mm statique HX (X=123Sb–31P), T° : -120°C +150°C ;
  • 7mm :
    • HX (X=207Pb–31P),
    • HX MQMAS (X=87Sr–93Nb).

REDORBOX, combined with a 4mm HX probe, enables correlations between nuclei at frequencies close to 100MHz, such as 13C, 27Al, 23Na or 51V.

For temperature control: BCU05, BCU X'trem and nitrogen evaporator.

Available probeheads:

  • 1,3mm HX (H=19F–1H ; X=14N–31P) ;
  • 1.6mm PhoenixNMR HXY (H=19F–1H ; X=29Si–31P, Y=109Ag–27Al), T° control (-60°C to +120°C), MAS < 40kHz
  • 2,5mm tri-Gamma® HXY (X=13C–31P ; Y=15N–29Si) ;
  • 3,2mm :
    • HX (X=15N–31P) ;
    • HX (X=183W–65Cu) ;
    • XY (X=31P ; Y=71Ga,11B,115Sn,87Rb), VESPEL stator (without 11B) ;
    • tri-Gamma® HXY (X=13C ; Y=14N) ;
    • tri-Gamma® HXY (X=11B ; Y=29Si) ;
    • tri-Gamma® HXY (X=13C–31P ; Y=15N–29Si) ;
    • HXY (X=31P, Y=93Nb, 51V–27Al) ;
    • PhoenixNMR HXY (H=19F–1H, X=29Si–31P, Y=109Ag–27Al), T°control (-30°C to +120°C), MAS < 25kHz
  • 4mm HX (X=183W–65Cu), rotor Revolution NMR type.
  • static 3 and 4 mm HX (X=197Au-125Te)

REDORBOX, combined with a 3.2mm HX probe, enables correlations between nuclei at frequencies close to 200MHz, such as 13C, 27Al, 23Na or 51V.

For temperature control: BCU 02 and nitrogen evaporator.

Available probeheads:

  • 1,3mm HX (X=14N–31P) ;

  • 2,5mm HX (X=14N–31P) ;

  • 3,2mm HCN ;

  • 7mm HX (X=143Nd–15N).

For temperature control: BCU 02.

Available probeheads:

  • 0,7mm DVT HCN (1H/13C/15N)
  • 1,3mm DVT HX (1H/103Rh-11B)
  • 3,2mm DVT HX (1H/103Rh-11B)