Solid-state NMR

Shared probeheads on both units:

• 1.3 mm HXY (X=¹³C–³¹P ; Y=¹⁸³W–¹¹B);
• 2.5 mm:
  • HX (¹H–¹⁹F ; X=¹¹³In–³¹P);
  • HXY (X=²⁹Si–³¹P ; Y=⁴⁷Ti–⁸⁷Rb);
• 3.2 mm HXY (X=¹¹¹Cd–³¹P ; Y=⁶⁷Zn–¹⁴¹Pr);
• 4 mm:
  • HX (X=²⁰⁷Pb–³¹P),
  • HX MQMAS (X=²⁹Si–¹¹⁹Sn),
  • HX (X=¹⁰⁵Pd–¹³C),
  • HX (¹⁰¹Ru–³¹P), WVT, T° : -60°C +300°C,
  • HX (X=⁷⁵As–³¹P ; Y=²⁵Mg–¹¹⁹Sn);
• 5 mm statique HX (X=¹²³Sb–³¹P), T° : -120°C +150°C;
• 7 mm:
  • HX (X=²⁰⁷Pb–³¹P),
  • HX MQMAS (X=⁸⁷Sr–⁹³Nb).

REDORBOX, combined with a 4 mm HX probe, enables correlations between nuclei at frequencies close to 100 MHz, such as ¹³C, ²⁷Al, ²³Na or ⁵¹V.

For temperature control: BCU05, BCU X'trem and nitrogen evaporator.

Available probeheads:

• 1.3 mm HX (H=¹⁹F–¹H ; X=¹⁴N–³¹P);
• 1.6 mm PhoenixNMR HXY (H=¹⁹F–¹H ; X=²⁹Si–³¹P, Y=¹⁰⁹Ag–²⁷Al), T° control (-60°C to +120°C), MAS < 40 kHz
• 2.5 mm tri-Gamma® HXY (X=¹³C–³¹P ; Y=¹⁵N–²⁹Si);
• 3.2 mm:
  • HX (X=¹⁵N–³¹P);
  • HX (X=¹⁸³W–⁶⁵Cu);
  • XY (X=³¹P ; Y=⁷¹Ga,¹¹B,¹¹⁵Sn,⁸⁷Rb), VESPEL stator (without ¹¹B);
  • tri-Gamma® HXY (X=¹³C ; Y=¹⁴N);
  • tri-Gamma® HXY (X=¹¹B ; Y=²⁹Si);
  • tri-Gamma® HXY (X=¹³C–³¹P ; Y=¹⁵N–²⁹Si);
  • HXY (X=³¹P, Y=⁹³Nb, ⁵¹V–²⁷Al);
  • PhoenixNMR HXY (H=¹⁹F–¹H, X=²⁹Si–³¹P, Y=¹⁰⁹Ag–²⁷Al), T°control (-30°C to +120°C), MAS < 25 kHz.
• 4 mm HX (X=¹⁸³W–⁶⁵Cu), rotor Revolution NMR type.
• static 3 and 4 mm HX (X=¹⁹⁷Au-¹²⁵Te).

REDORBOX, combined with a 3.2 mm HX probe, enables correlations between nuclei at frequencies close to 200 MHz, such as ¹³C, ²⁷Al, ²³Na or ⁵¹V.

For temperature control: BCU 02 and nitrogen evaporator.

Available probeheads:

• 1.3 mm HX (X=¹⁴N–³¹P);

• 2.5 mm HX (X=¹⁴N–³¹P);

• 3.2 mm HCN;

• 7 mm HX (X=¹⁴³Nd–¹⁵N).

For temperature control: BCU 02.

Available probeheads:

• 0.7 mm DVT HCN (¹H/¹³C/¹⁵N)
• 1.3 mm DVT HX (¹H/¹⁰³Rh-¹¹B)
• 3.2 mm DVT HX (¹H/¹⁰³Rh-¹¹B)